HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum isopropoxide → HCID 14691048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum isopropoxide | HCID 11143 | — |
| Reactant | 1-Methyl-2-(2,2-dimethyl-2-formylethyl)-3-isopropenylcyclopent-1-ene | HCID 5014262 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 14691048 | HCID 14691048 | — |
Reaction Steps
103 g (0.5 mole) of the product from Example 1 were reduced with 60 g of isopropanol and 20 g of aluminum triisopropylate by the Meerwein-Ponndorf method. The conversion was 78% and the yield of the above compound (for characteristics thereof, see Example 3), based on the above conversion, was 73%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04069258 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-93ca427e89314dd5bef9a8e4295c5a51 |
| Source note | uspto-grants-1978_01 |