HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22749369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl N-methyl-5-nitro-N-[tris(hydroxymethyl)methyl]isophthalamate | HCID 22749370 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22749369 | HCID 22749369 | — |
Reaction Steps
Methyl N-methyl-5-nitro-N-[tris(hydroxymethyl)methyl]isophthalamate is stirred with one equivalent of sodium hydroxide in aqueous methanol. The reaction mixture is concentrated to remove the methanol, diluted with water and acidified with mineral acid to provide crystalline N-methyl-5-nitro-N-[tris (hydroxymethyl)methyl]isophthalamic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04069250 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-03a4d7f21d94406da5dbe5005ae1f081 |
| Source note | uspto-grants-1978_01 |