HuagongsheHuagongshe Chemistry Print Report · For research reference only
O,O-diethyl phosphorochloridothioate → HCID 12526293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O,O-diethyl phosphorochloridothioate | HCID 17305 | — |
| Reactant | HCID 178483103 | HCID 178483103 | — |
| Product | HCID 12526293 | HCID 12526293 | — |
Reaction Steps
Using the procedure of Example 6, diethyl chlorothiophosphate and 3 -hydroxy-5-dimethylamino-1,2,4-thiadiazole were reacted and after chromatography and elution with an 8-2benzene-ethylacetate mixture, there was obtained 3-(diethoxythiophosphoryloxy)-5-dimethylamino-1,2,4-thiadiazole with a melting point of 48° C and Rf=0.55.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04069319 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-41a133b378194175818d37621db2e513 |
| Source note | uspto-grants-1978_01 |