Hydrogen Peroxide → HCID 178425939, compound

HRID 1834191Notes

Reaction equation

HRID 1834191 reaction equation
[C:1]([N:3]=[C:4]([S-:6])[S-:5])#[N:2].[K+].[K+].[CH3:9][C:10]1[CH:17]=[CH:16][C:13]([CH2:14]Cl)=[CH:12][CH:11]=1.[OH:18]O>>[OH:18][C:1]1[N:3]=[C:4]([S:6][CH2:9][C:10]2[CH:17]=[CH:16][C:13]([CH3:14])=[CH:12][CH:11]=2)[S:5][N:2]=1

Participants

4

Reactant 3

HCID 784Hydrogen PeroxideHCID 77224-Methylbenzyl chlorideHCID 83179Carbamodithioic acid, cyano-, dipotassium salt

Product 1

HCID 178425939HCID 178425939, compound

Procedure

Using the procedure of Example 12, 58.2 g of dipotassium N-cyanodithioimidocarbonate and 42 g of p-methylbenzyl chloride were reacted and then were treated with 35 ml of 30% hydrogen peroxide to obtain 26 g of 3-hydroxy-5-p-methylbenzylthio-1,2,4-thiadiazole melting at 144° C.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-62dd95941a1746b7afdac4b9bf9ed2d8
Source dataset
uspto-grants-1978_01
Patent number
US04069319

Reaction notes

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