Paraldehyde → HCID 15818775, compound

HRID 1834426Notes

Reaction equation

HRID 1834426 reaction equation
[CH2:1]([C:3]1[C:7]([CH3:8])=[C:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[NH:5][CH:4]=1)[CH3:2].[CH3:14][CH:15]1OC(C)OC(C)O1>>[CH2:14]([C:4]1[NH:5][C:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])=[C:7]([CH3:8])[C:3]=1[CH2:1][CH3:2])[CH3:15]

Participants

3

Reactant 2

HCID 31264ParaldehydeHCID 14057066HCID 14057066, compound

Product 1

HCID 15818775HCID 15818775, compound

Procedure

As in Example 32 but using 3-ethyl-4-methyl-5-carbethoxy-pyrrole and paraldehyde. Colourless prisms (64%), m.p. 71°-73° (lit. 8) 73°-74°). Anal. Calc. for C12H19NO2 : C, 68.86; H, 9.15; N, 6.67. Found: C, 68.71; H, 9.11; N, 6.84.

Sources & evidence

ORD record
ord-725b6789f7ea4a9ebde5628a949ac643
Source dataset
uspto-grants-1978_01
Patent number
US04070366

Reaction notes

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