HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 15711941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2,5-Dimethylpyrrole | HCID 12265 | — |
| Reactant | Hydrogen iodide | HCID 24841 | — |
| Reactant | Paraldehyde | HCID 31264 | — |
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Product | HCID 15711941 | HCID 15711941 | — |
Reaction Steps
As in Example 58, using 2,5-dimethyl-pyrrole (2g), acetic acid (50 ml), hydriodic acid (50 ml), hypophosphorous acid (10 ml) and paraldehyde (1.4 ml). The product (46%) was an oil, b.p. 48°-50° (0.05 mm). Anal. Calc. for C10H17N: C, 79.40; H, 11.34; N, 9.26. Found: C, 79.21; H, 11.53; N, 9.09.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04070366 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-0067c9bf44184956892ac67a7291b5a9 |
| Source note | uspto-grants-1978_01 |