Potassium Carbonate → HCID 178433288, compound

HRID 1834559Notes

Reaction equation

HRID 1834559 reaction equation
C(=O)([O-])[O-].[K+].[K+].Cl.Cl.[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]>O>[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 30159992-(((5-Methyl-1H-imidazol-4-yl)methyl)thio)ethylamine dihydrochloride

Product 1

HCID 178433288HCID 178433288, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Potassium carbonate (7.75 g.) was added to a solution of 4-methyl-5-[(2-aminoethyl)thiomethyl]-imidazole dihydrochloride (14.6 g.) in water (120 ml.). The solution was stored at room temperature for 15 minutes, then evaporated to dryness, extracted with isopropyl alcohol and the extracts are concentrated to dryness to give 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole.

Workup

  1. customevaporated to dryness
  2. extractionextracted with isopropyl alcohol
  3. concentrationthe extracts are concentrated to dryness

Sources & evidence

ORD record
ord-ceb1dd078eef417fb4c012a5e0881382
Source dataset
uspto-grants-1978_01
Patent number
US04070475

Reaction notes

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