Chlorine → HCID 20373880, compound

HRID 1834695Notes

Reaction equation

HRID 1834695 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([OH:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][CH:3]1[CH3:18].[Cl:19]Cl>Cl.C(O)(=O)C>[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([OH:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:18])[Cl:19]

Participants

5

Reactant 2

HCID 24526ChlorineHCID 33795[(6,7-Dichloro-2-methyl-1-oxo-2,3-dihydro-1H-inden-5-yl)oxy]acetic acid

Product 1

HCID 20373880HCID 20373880, compound

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidCatalystHCID 176Acetic AcidSolvent

Procedure

By following substantially the procedure described in Example 12, Step B, and using as the reactants (1-oxo-2-methyl-6,7-dichloro-5-indanyloxy)acetic acid (2.89 g., 0.01 mole), glacial acetic acid (50 ml.), chlorine (710 mg., 0.01 mole) and concentrated hydrochloric acid (1 drop) there is obtained (1-oxo-2-methyl-2,6,7-trichloro-5-indanyloxy)acetic acid.

Sources & evidence

ORD record
ord-37cea8f5cf8345b4a5ab7b58c6e9e5c3
Source dataset
uspto-grants-1978_01
Patent number
US04070539

Reaction notes

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