Methyl Isocyanate → HCID 53643193, compound

HRID 1834883Notes

Reaction equation

HRID 1834883 reaction equation
[N:1](=[C:3]1[CH:8]([CH3:9])[N:7]([CH3:10])[C:6](=[O:11])[CH2:5][S:4]1)[OH:2].[CH3:12][N:13]=[C:14]=[O:15]>C(N(CC)CC)C>[CH3:12][NH:13][C:14]([O:2][N:1]=[C:3]1[CH:8]([CH3:9])[N:7]([CH3:10])[C:6](=[O:11])[CH2:5][S:4]1)=[O:15]

Participants

4

Reactant 2

HCID 12228Methyl IsocyanateHCID 85945283HCID 85945283, compound

Product 1

HCID 53643193HCID 53643193, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Utilizing the procedure of Example V, 2-oximino-3,4-dimethyltetrahydro-1,4-thiazin-5-one was reacted with methyl isocyanate in the presence of triethylamine to yield 3 g of 2-[O-(methylcarbamoyl)oximino]-3,4-dimethyltetrahydro-1,4-thiazin-5-one, m.p. 161°-163° C.

Sources & evidence

ORD record
ord-38d5b3f112174e42b41fe575c393df24
Source dataset
uspto-grants-1978_01
Patent number
US04071627

Reaction notes

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