(Aminooxy)acetic acid → HCID 54368970, compound

HRID 1834903Notes

Reaction equation

HRID 1834903 reaction equation
[CH3:1][C:2]([C:4]1[CH:9]=[CH:8][C:7]([Cl:10])=[C:6]([Cl:11])[CH:5]=1)=O.[NH2:12][O:13][CH2:14][C:15]([OH:17])=[O:16].C([O-])(=O)C.[Na+]>C(O)C>[CH3:1][C:2](=[N:12][O:13][CH2:14][C:15]([OH:17])=[O:16])[C:4]1[CH:9]=[CH:8][C:7]([Cl:10])=[C:6]([Cl:11])[CH:5]=1

Participants

5

Reactant 3

HCID 286(Aminooxy)acetic acidHCID 75841Ethanone, 1-(3,4-dichlorophenyl)-HCID 517045Sodium Acetate

Product 1

HCID 54368970HCID 54368970, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In the manner described in example 1, the above substance was obtained by boiling 4.73 g or 3,4-dichloroacetophenone, 2.74 g of hemihydrochloride of aminooxyacetic acid and 6.15 g of sodium acetate in 80% ethanol for one hour. After one crystallisation from a mixture of benzene and petroleum ether, the melting point was 128°-129° C.

Workup

  1. customthe above substance was obtained
  2. customfor one hour
  3. customAfter one crystallisation
  4. additionfrom a mixture of benzene and petroleum ether

Sources & evidence

ORD record
ord-b3456fcf8c734279a8b1de10c063d807
Source dataset
uspto-grants-1978_01
Patent number
US04071686

Reaction notes

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