HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Aminooxy)acetic acid → HCID 54368970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Aminooxy)acetic acid | HCID 286 | — |
| Reactant | Ethanone, 1-(3,4-dichlorophenyl)- | HCID 75841 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54368970 | HCID 54368970 | — |
Reaction Steps
In the manner described in example 1, the above substance was obtained by boiling 4.73 g or 3,4-dichloroacetophenone, 2.74 g of hemihydrochloride of aminooxyacetic acid and 6.15 g of sodium acetate in 80% ethanol for one hour. After one crystallisation from a mixture of benzene and petroleum ether, the melting point was 128°-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04071686 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-b3456fcf8c734279a8b1de10c063d807 |
| Source note | uspto-grants-1978_01 |