Triethylamine → HCID 54141893, compound

Participants

Reaction Steps

In general analogy to the process described under 1.2, 27.7 g (0.157 mol) of α-hydroxyimino-3-methoxybenzylcyanide are reacted in the presence of 23.9 g (0.236 mol) of triethylamine with 19.8 g (0.173 mol) of methanesulfonyl chloride. Recrystallisation from toluene gives 19.1 g (48%) of α-(methylsulfonyloxyimino)-3-methoxybenzylcyanide in the form of white crystals having an m.p. of 105-107° C.

Provenance & Evidence