Ethanol → HCID 69303462, compound

Participants

Reaction Steps

The reaction was carried out in exactly the same manner as Reference Example 6 using 37 g of the (1S,6R)-2,2,6-trimethylcyclohexyl methyl ketone (1a) synthesized in Example 2 to obtain 29 g of (1S,6R)-1-(2,2,6-trimethylcyclohexyl)-2-buten-1-one (10a) (b.p.: 73-75° C./19.95 Pa (0.15 torr), [α]D=+15.52° (c 1.00, EtOH, 24° C.).

Provenance & Evidence