HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23500354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phloroglucinol | HCID 359 | — |
| Reactant | Ethyl 2-oxo-5-phenylcyclohexane-1-carboxylate | HCID 23500357 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23500354 | HCID 23500354 | — |
Reaction Steps
A solution of phloroglucinol (1.56 g) and ethyl 2-oxo-5-phenylcyclo-hexane-carboxylate (2.52 g) in ethanol (25 ml) was treated with dry HCl as described in example 1a. The precipitate was filtered and washed with water and ETOH. Yield 1.0 g (32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774103B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-9554ac6dddb6465a8126fd7a2cd158a1 |
| Source note | uspto-grants-2004_08 |