Hydrochloric Acid → HCID 23500354, compound

HRID 1835681Notes

Reaction equation

HRID 1835681 reaction equation
[C:1]1([CH:9]=[C:7]([OH:8])[CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].O=[C:11]1[CH2:16][CH2:15][CH:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][CH:12]1[C:23](OCC)=[O:24].Cl>C(O)C>[OH:2][C:1]1[C:9]2[C:11]3[CH2:16][CH2:15][CH:14]([C:17]4[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH2:13][C:12]=3[C:23](=[O:24])[O:8][C:7]=2[CH:6]=[C:4]([OH:5])[CH:3]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 359PhloroglucinolHCID 23500357Ethyl 2-oxo-5-phenylcyclohexane-1-carboxylate

Product 1

HCID 23500354HCID 23500354, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of phloroglucinol (1.56 g) and ethyl 2-oxo-5-phenylcyclo-hexane-carboxylate (2.52 g) in ethanol (25 ml) was treated with dry HCl as described in example 1a. The precipitate was filtered and washed with water and ETOH. Yield 1.0 g (32%).

Workup

  1. filtrationThe precipitate was filtered
  2. washwashed with water and ETOH

Sources & evidence

ORD record
ord-9554ac6dddb6465a8126fd7a2cd158a1
Source dataset
uspto-grants-2004_08
Patent number
US06774103B1

Reaction notes

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