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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1835768Generated: November 1, 2026

Acetyl chloride → HCID 23500854, compound

https://huagongshe.com/reaction/1835768

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetyl chlorideHCID 6367—
ReactantMorpholineHCID 8083—
Reactant2-MethoxybenzaldehydeHCID 8658—
ProductHCID 23500854HCID 23500854—

Reaction Steps

The reaction of 8.5 g (0.100 mol) morpholine and 7.0 g (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.1 g (corresponding to 58% of the yield calculated by theory) 4-(2-methyl-benzylidene)-morpholin-4-ium chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06774136B2
Source datasetuspto-grants-2004_08
ORD IDord-e31dd4fc2a1e458796e236e068312818
Source noteuspto-grants-2004_08