HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 23500854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Product | HCID 23500854 | HCID 23500854 | — |
Reaction Steps
The reaction of 8.5 g (0.100 mol) morpholine and 7.0 g (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 7.1 g (corresponding to 58% of the yield calculated by theory) 4-(2-methyl-benzylidene)-morpholin-4-ium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774136B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-e31dd4fc2a1e458796e236e068312818 |
| Source note | uspto-grants-2004_08 |