2-Naphthol → HCID 23500858, compound

HRID 1835792Notes

Reaction equation

HRID 1835792 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[OH:11].[Cl-].[CH:13](=[N+:20]([CH3:22])[CH3:21])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[CH3:23][O:24][C:25]1[CH:32]=[CH:31][C:28]([CH2:29]Cl)=[CH:27][CH:26]=1>>[CH3:23][O:24][C:25]1[CH:32]=[CH:31][C:28]([CH2:29][O:11][C:2]2[CH:3]=[CH:4][C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[C:1]=2[CH:13]([N:20]([CH3:22])[CH3:21])[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:27][CH:26]=1

Participants

4

Reactant 3

HCID 86632-NaphtholHCID 699934-Methyloxybenzyl chlorideHCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

Product 1

HCID 23500858HCID 23500858, compound

Procedure

The preparation was carried out in accordance with general synthesis instructions 4 and 5 from 2-naphthol, benzylidene-dimethyl-ammonium chloride and 4-methoxybenzyl chloride. The structure was demonstrated by means of ESI-MS: mass calculated 397.52 g/mol, mass found M+H=398.0.

Sources & evidence

ORD record
ord-3f2f7545f89348ef820022ae780e69c5
Source dataset
uspto-grants-2004_08
Patent number
US06774136B2

Reaction notes

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