HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4,6-Difluoroaniline → HCID 23500738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4,6-Difluoroaniline | HCID 136285 | — |
| Reactant | 1-benzyl-1,2,5,6-tetrahydropyridine-3-carboxylic acid methyl ester | HCID 11447585 | — |
| Reactant | HCID 23500666 | HCID 23500666 | — |
| Solvent | HCID 86592183 | HCID 86592183 | — |
| Product | HCID 23500738 | HCID 23500738 | — |
Reaction Steps
1-Benzyl-N-(2-bromo-4,6-difluorophenyl)-1,2,5,6-tetrahydropyridine-3-carboxamide. The title compound was prepared from 2-bromo-4,6-difluoroaniline and 1-benzyl-1,2,5,6-tetrahydropyridine-3-carboxylic acid methyl ester as described in EXAMPLE 1. Rf 0.53 (toluene/acetonitrile/tri-ethyl amine 10:10:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774132B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-e805801351a14279b508cdb7f0e5985c |
| Source note | uspto-grants-2004_08 |