HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 9859441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | HCID 9859066 | HCID 9859066 | — |
| Product | HCID 9859441 | HCID 9859441 | — |
Reaction Steps
The compound was prepared according to PROCEDURE 1, Method A by reaction with spiro[indoline-3,3′-piperidin]-2-one and acetaldehyde (5 equivalents). Yield: 45 mg (26%). 13C NMR of the HCl-salt (CD3OD): δ 9.6, 19.8, 31.3, 46.3, 54.2, 54.3, 55.1, 111.5, 123.9, 124.4, 130.4, 131.3, 142.6, 182.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774132B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-35ef0cf993d24348a2b86873d8a86571 |
| Source note | uspto-grants-2004_08 |