HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 9816288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Methane | HCID 297 | — |
| Reactant | HCID 9859066 | HCID 9859066 | — |
| Product | HCID 9816288 | HCID 9816288 | 75% |
Reaction Steps
The compound was prepared according to PROCEDURE 1, Method A by reaction with spiro[indoline-3,3′-piperidin]-2-one and acetone (5 equivalents). Yield: 75%. 13C NMR (CDCl3): δ 17.6, 17.7, 21.7, 32.1, 48.6, 48.8, 54.0, 54.8, 109.6, 121.6, 126.2, 127.2, 134.8, 140.1, 182.4; MS (CI, CH4): m/z (rel. int.) 245 (M+1, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774132B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-3a3ba5884ea0404f9109ac92f6373b8d |
| Source note | uspto-grants-2004_08 |