HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 10131020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | HCID 9859066 | HCID 9859066 | — |
| Product | HCID 10131020 | HCID 10131020 | — |
Reaction Steps
The compound was prepared according to PROCEDURE 1, Method B by reaction of spiro[indoline-3,3′-piperidin]-2-one with allyl bromide (1.1 equivalents). 13C NMR (CDCl3): δ 21.2, 31.3, 48.4, 53.3, 58.1, 61.6, 109.5, 117.2, 121.6, 125.7, 127.4, 134.3, 135.1, 140.0, 181.6; MS (CI, CH4): m/z (rel. int.) 243 (M+1, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774132B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-33e19eb38b43454dbd406c964c385592 |
| Source note | uspto-grants-2004_08 |