Methane → HCID 10131020, compound

HRID 1835847Notes

Reaction equation

HRID 1835847 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][C:3]2([C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[NH:8][C:7]2=[O:15])[CH2:2]1.[CH2:16](Br)[CH:17]=[CH2:18].C>>[CH2:18]([N:1]1[CH2:6][CH2:5][CH2:4][C:3]2([C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[NH:8][C:7]2=[O:15])[CH2:2]1)[CH:17]=[CH2:16]

Participants

4

Reactant 3

HCID 297MethaneHCID 7841Allyl bromideHCID 9859066HCID 9859066, compound

Product 1

HCID 10131020HCID 10131020, compound

Procedure

The compound was prepared according to PROCEDURE 1, Method B by reaction of spiro[indoline-3,3′-piperidin]-2-one with allyl bromide (1.1 equivalents). 13C NMR (CDCl3): δ 21.2, 31.3, 48.4, 53.3, 58.1, 61.6, 109.5, 117.2, 121.6, 125.7, 127.4, 134.3, 135.1, 140.0, 181.6; MS (CI, CH4): m/z (rel. int.) 243 (M+1, 100).

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-33e19eb38b43454dbd406c964c385592
Source dataset
uspto-grants-2004_08
Patent number
US06774132B1

Reaction notes

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