HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 9881552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Cyclopropanecarboxaldehyde | HCID 123114 | — |
| Reactant | HCID 9859066 | HCID 9859066 | — |
| Product | HCID 9881552 | HCID 9881552 | 90% |
Reaction Steps
The compound was prepared according to PROCEDURE 1, Method A by reaction of spiro[indoline-3,3′-piperidin]-2-one with 3 equiv. of cyclopropanecarboxaldehyde. Yield: 90%. 13C NMR (CDCl3): δ 3.8, 4.0, 8.3, 21.4, 31.8, 48.6, 53.3, 58.4, 63.6, 109.7, 121.7, 126.1, 127.4, 134.7, 140.0, 182.2; MS (CI, CH4): m/z (rel. int.) 257 (M+1, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774132B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-55731c172748454598d4f54a65c54750 |
| Source note | uspto-grants-2004_08 |