HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 23500704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | HCID 9859066 | HCID 9859066 | — |
| Product | HCID 23500704 | HCID 23500704 | 46% |
Reaction Steps
The compound was prepared according to PROCEDURE 1, Method A by reaction with spiro[indoline-3,3′-piperidin]-2-one and 2-butanone (3 equivalents). Yield: 46%. 13C NMR (CDCl3): δ 11.5, 11.6, 13.3, 13.3, 21.7, 21.9, 26.4, 26.5, 32.1, 32.1, 46.1, 48.6, 49.0, 50.9, 52.4, 56.6, 61.2, 62.5, 109.6, 121.5, 121.6, 126.4, 126.5, 127.2, 134.7, 134.9, 140.1, 140.1, 182.4, 182.5; MS (CI, CH4): m/z (rel. int.) 259 (M+1, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06774132B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-8bb57af6ad5344dda5350f1569430535 |
| Source note | uspto-grants-2004_08 |