Hydrochloric Acid → HCID 23500684, compound

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Reaction Steps

(S)-Spiro[indoline-3,3′-(1,3,4,7-tetrahydro-2H-azepin)]-2-one Hydrochloride The material from the second peak from STEP C (47 mg) was dissolved in methanol (5 ml) and treated with HCl in ether (1.5 ml) at room temperature overnight. The title compound was obtained upon removal of solvents. MS (TSP+) m/z [M+H]+: 215. 13C NMR: (CD3OD): 181.0, 142.1, 132.7, 132.2, 130.4, 125.7, 124.8, 123.8, 111.6, 53.8, 47.6, 47.5, 35.4 ppm.

Provenance & Evidence