HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23518325, compound → HCID 23518327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23518325 | HCID 23518325 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 23518327 | HCID 23518327 | 100.6% |
Reaction Steps
A mixture of the compound from Step F (0.27 g, 0.53 mmol) and methanolic ammonia (saturated at 0° C.; 10 mL) was kept overnight at 0° C. Evaporation of the solvent yielded the desired compound (0.25 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777395B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-1a3fe742a3eb48b8826c620b8461b14e |
| Source note | uspto-grants-2004_08 |