HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23499226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12049569 | HCID 12049569 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23499226 | HCID 23499226 | 74.6% |
Reaction Steps
The compound of Example 2 (200 mg) was dissolved in 2 ml of tetrahydrofuran, and 2 ml of 2N hydrochloric acid was added. After overnight stirring at room temperature, the reaction mixture was filtered under reduced pressure. The resulting solid was dried in a vacuum to obtain 119 mg of the title compound. Its physical properties are shown below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777427B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-7d6cdf4729c44d75b3417a676ad2fb5c |
| Source note | uspto-grants-2004_08 |