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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1836310Generated: October 28, 2026

Hydrochloric Acid → HCID 23499226, compound

https://huagongshe.com/reaction/1836310

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 12049569HCID 12049569—
SolventTetrahydrofuranHCID 8028—
ProductHCID 23499226HCID 2349922674.6%

Reaction Steps

The compound of Example 2 (200 mg) was dissolved in 2 ml of tetrahydrofuran, and 2 ml of 2N hydrochloric acid was added. After overnight stirring at room temperature, the reaction mixture was filtered under reduced pressure. The resulting solid was dried in a vacuum to obtain 119 mg of the title compound. Its physical properties are shown below.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06777427B2
Source datasetuspto-grants-2004_08
ORD IDord-7d6cdf4729c44d75b3417a676ad2fb5c
Source noteuspto-grants-2004_08