HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 12727037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 23499332 | HCID 23499332 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 12727037 | HCID 12727037 | 91.3% |
Reaction Steps
A mixture of 4-[3-methoxybenzoyl]pyridine(790 mg, 3.7 mmol) and iodomethane (1.15 ml, 18.5 mmol) in acetone (10 mL) was stirred at room temperature for 48 h. The precipitate was filtered, washed with diethyl ether and dried in vacuo to give 1.2 g (91%) of an orange powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777428B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-7505b758e81548c987d0decc5c2067d6 |
| Source note | uspto-grants-2004_08 |