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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1836350Generated: November 3, 2026

Methyl iodide → HCID 12727037, compound

https://huagongshe.com/reaction/1836350

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 23499332HCID 23499332—
SolventAcetoneHCID 180—
ProductHCID 12727037HCID 1272703791.3%

Reaction Steps

A mixture of 4-[3-methoxybenzoyl]pyridine(790 mg, 3.7 mmol) and iodomethane (1.15 ml, 18.5 mmol) in acetone (10 mL) was stirred at room temperature for 48 h. The precipitate was filtered, washed with diethyl ether and dried in vacuo to give 1.2 g (91%) of an orange powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06777428B1
Source datasetuspto-grants-2004_08
ORD IDord-7505b758e81548c987d0decc5c2067d6
Source noteuspto-grants-2004_08