HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 86759507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 86759508 | HCID 86759508 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86759507 | HCID 86759507 | 76.9% |
Reaction Steps
4-[3-(methylamidyl)benzoyl]-1-methylpiperidine (283 mg, 1.1 mmol) in ethyl acetate was added to oxalic acid (99 mg, 1.1 mmol) in ethyl acetate. The resulting precipitate was filtered, washed with ethyl acetate, and dried under vacuum to give 270 mg (71%) of tan powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777428B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-2c33df228b9c46bea9b9ff598e7f534f |
| Source note | uspto-grants-2004_08 |