HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzoyl chloride → 4-[3-(2-Methoxybenzamidyl)benzoyl]-1-methylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Reactant | 4-[3-Aminobenzoyl]-1-methylpiperidine | HCID 10130651 | — |
| Product | 4-[3-(2-Methoxybenzamidyl)benzoyl]-1-methylpiperidine | HCID 23518814 | 78% |
Reaction Steps
Beginning with 4-[3-aminobenzoyl]-1-methylpiperidine (50 mg, 0.229 mmol) and 2-methoxybenzoyl chloride (102 μl, 0.685 mmol), 62.6 mg (78%) of the title compound were recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777428B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-d549d9fee97d411eaf7a586bbe6b95db |
| Source note | uspto-grants-2004_08 |