HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,6-Trifluorobenzoyl chloride → 4-[3-(2,3,6-Trifluorobenzamidyl)benzoyl]-1-methylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,6-Trifluorobenzoyl chloride | HCID 594407 | — |
| Reactant | 4-[3-Aminobenzoyl]-1-methylpiperidine | HCID 10130651 | — |
| Product | 4-[3-(2,3,6-Trifluorobenzamidyl)benzoyl]-1-methylpiperidine | HCID 69355853 | — |
Reaction Steps
Beginning with 4-[3-aminobenzoyl]-1-methylpiperidine (25 mg, 0.115 mmol) and 2,3,6-trifluorobenzoyl chloride (30 μL, 0.229 mmol) and mixing for 24 h, 47.7 mg (>100%) of the title compound were recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777428B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-293c6530f70b47c98dd51f9e9dad59f5 |
| Source note | uspto-grants-2004_08 |