Phenyl Isothiocyanate → HCID 86759509, compound

HRID 1836405Notes

Reaction equation

HRID 1836405 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=1)[C:5]([CH:7]1[CH2:12][CH2:11][N:10]([CH3:13])[CH2:9][CH2:8]1)=[O:6].[C:17]1([N:23]=[C:24]=[S:25])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:17]1([NH:23][C:24](=[S:25])[NH:1][C:2]2[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=2)[C:5]([CH:7]2[CH2:8][CH2:9][N:10]([CH3:13])[CH2:11][CH2:12]2)=[O:6])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 7673Phenyl IsothiocyanateHCID 101306514-[3-Aminobenzoyl]-1-methylpiperidine

Product 1

HCID 86759509HCID 86759509, compoundYield 100%

Procedure

Beginning with 4-[3-aminobenzoyl]-1-methylpiperidine (25 mg, 0.115 mmol) and phenyl isothiocyanate (82 μL, 0.688 mmol), 40.5 mg (100%) of the title compound were recovered.

Sources & evidence

ORD record
ord-3b0d6356d3f54acf9c5755ac2689d62e
Source dataset
uspto-grants-2004_08
Patent number
US06777428B1

Reaction notes

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