HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 2653166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 2653166 | HCID 2653166 | — |
Reaction Steps
To a suspension of 6-chloronicotinoyl chloride (10.5 g, 59.7 mmole) in dry dichloromethane (100 mL) was added 4-fluoroaniline (5.6 mL, 59.7 mmole), followed by the dropwise addition of N,N-diisopropylethylamine (21 mL, 19 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06777432B1 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-9ef1827f3fcf4acfa22c08a05c25714b |
| Source note | uspto-grants-2004_08 |