HCID 9902505, compound → HCID 10788351, compound

HRID 1836802Notes

Reaction equation

HRID 1836802 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:11]([C:13]2[CH:14]=[C:15]([O:23][CH3:24])[C:16]([O:21][CH3:22])=[C:17]([O:19][CH3:20])[CH:18]=2)=[O:12])=[C:7]([OH:10])[C:8]=1[OH:9]>CO>[CH3:1][O:2][CH2:3][O:10][C:7]1[C:8]([O:9][CH2:17][O:19][CH3:20])=[C:3]([O:2][CH3:1])[CH:4]=[CH:5][C:6]=1[C:11](=[O:12])[C:13]1[CH:14]=[C:15]([O:23][CH3:24])[C:16]([O:21][CH3:22])=[C:17]([O:19][CH3:20])[CH:18]=1

Participants

3

Reactant 1

HCID 9902505HCID 9902505, compound

Product 1

HCID 10788351HCID 10788351, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

X-Ray Crystal Structure Determination of Hydroxyphenstatin (6a). A thick, plate-shaped X-ray sample (˜0.38×0.36×0.08 mm), grown from methanol solution, was mounted on the tip of a glass fiber with Super-Glue. Data collection was performed at 301±1° K. Accurate cell dimensions were determined by least-squares fitting of 25 carefully centered reflections in the range of 35°<è<40° using Cu Ká radiation.

Workup

  1. customData collection
  2. customwas performed at 301±1° K
  3. customby least-squares fitting of 25 carefully centered reflections in the range of 35°<è<40°

Sources & evidence

ORD record
ord-71e06b863fc04558a70525bef14ecadb
Source dataset
uspto-grants-2004_08
Patent number
US06777578B2

Reaction notes

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