2-Naphthoic acid → HCID 7927248, compound

HRID 1837151Notes

Reaction equation

HRID 1837151 reaction equation
[CH3:1][C:2]1[CH:6]=[CH:5][S:4][C:3]=1[C:7]([OH:9])=O.[I:10][C:11]1[CH:17]=[CH:16][C:14]([NH2:15])=[CH:13][CH:12]=1.C1C2C(=CC=CC=2)C=CC=1C(O)=O>>[I:10][C:11]1[CH:17]=[CH:16][C:14]([NH:15][C:7]([C:3]2[S:4][CH:5]=[CH:6][C:2]=2[CH3:1])=[O:9])=[CH:13][CH:12]=1

Participants

4

Reactant 3

HCID 71232-Naphthoic acidHCID 108934-Iodoaniline2×HCID 902693-Methyl-2-thenoic acid

Product 1

HCID 7927248HCID 7927248, compound

Procedure

This compound was synthesized by the same procedure as for Example 15, except 3-methyl-2-thiophenecarboxylic acid and 4-iodoaniline were used instead of 2-napthoic acid and 4-iodoaniline. M+1=344.2, mp 141˜142° C.

Sources & evidence

ORD record
ord-f646a4a819e640dd99b7e6a8f639063d
Source dataset
uspto-grants-2004_08
Patent number
US06780883B2

Reaction notes

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