HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21960150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(2-Bromoethoxy)Benzaldehyde | HCID 262706 | — |
| Reactant | HCID 135678130 | HCID 135678130 | — |
| Product | HCID 21960150 | HCID 21960150 | 40% |
Reaction Steps
The title compound (138 mg, 40%) was prepared from 2-ethyl-4-trifluoromethyl-1,6-dihydro-6-pyrimidone (200 mg, 1.04 mmol) and 4-[2-bromoethoxy]benzaldehyde (238.5 mg, 1.04 mmol) in presence of K2CO3 (287.5 mg, 2.08 mmol) as base by a similar procedure to that described in preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06780992B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-0873428c050940678b6fa117134bd5b2 |
| Source note | uspto-grants-2004_08 |