HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22677060, compound → HCID 22677059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22677060 | HCID 22677060 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22677059 | HCID 22677059 | — |
Reaction Steps
A suspension of compound 16 (18.18 g, 0.071 mol) and palladium hydroxide on charcoal (2.46 g, 2.13 mmol) in ethanol and ethyl acetate (120 ml, 1:1) was stirred under an atmosphere of hydrogen for 24 h at room temperature. The reaction mixture was filtered (celite) and the solvent roved in vacuo to yield a clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06783812B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-e2c3c2bb9e0b449ab5e8b4a1bcd90d4a |
| Source note | uspto-grants-2004_08 |