Hydrochloric Acid → HCID 178507240, compound

HRID 1837507Notes

Reaction equation

HRID 1837507 reaction equation
Cl.[N+:2]([C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[CH2:10][CH:9]([C:14]1[N:15]=[CH:16][NH:17][CH:18]=1)[CH2:8]2)([O-])=O>C(O)C.[Pd]>[NH:17]1[CH:18]=[C:14]([CH:9]2[CH2:8][C:7]3[C:11](=[CH:12][CH:13]=[C:5]([NH2:2])[CH:6]=3)[CH2:10]2)[N:15]=[CH:16]1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 178526436HCID 178526436, compound

Product 1

HCID 178507240HCID 178507240, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The hydrochloride of the product obtained in Step 3 is stirred under a hydrogen atmosphere in the presence of 10% palladium-on-carbon in ethanol. After filtration and concentration of the solvent, the product is used as it is in the following Step.

Workup

  1. filtrationAfter filtration and concentration of the solvent

Sources & evidence

ORD record
ord-242418fba3d34fc9b4850ed85f169832
Source dataset
uspto-grants-2004_08
Patent number
US06784183B2

Reaction notes

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