Hydrochloric Acid → HCID 178507552, compound

HRID 1837514Notes

Reaction equation

HRID 1837514 reaction equation
Cl.[N+:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]2[N:14]=[CH:15][NH:16][CH:17]=2)[CH:8]=[CH:9][CH:10]=1)([O-])=O>C(O)C.[Pd]>[NH:16]1[CH:17]=[C:13]([CH2:12][CH2:11][C:7]2[CH:6]=[C:5]([NH2:2])[CH:10]=[CH:9][CH:8]=2)[N:14]=[CH:15]1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 178526618HCID 178526618, compound

Product 1

HCID 178507552HCID 178507552, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The hydrochloride of the product obtained in Step 4 is stirred under a hydrogen atmosphere in the presence of a 90% solution of 10% palladium-on-carbon in ethanol. After filtration and concentration of the solvent, the product is used as it is in the following Step.

Workup

  1. filtrationAfter filtration and concentration of the solvent

Sources & evidence

ORD record
ord-c05f04d7445441999255cb7dde1119d8
Source dataset
uspto-grants-2004_08
Patent number
US06784183B2

Reaction notes

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