Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1837720Generated: November 2, 2026

HCID 22678362, compound → HCID 22678736, compound

https://huagongshe.com/reaction/1837720

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22678362HCID 22678362—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 22678736HCID 2267873698.4%

Reaction Steps

554 mg of 1-(benzyloxycarbonyl)-4-[(E)-2-[(2-cyclohexylmethyloxy)phenyl]-1-ethenyl]piperidine was dissolved in 10 ml of ethanol, 250 mg of 10% palladium-carbon powder (water-containing product) was added thereto, and the mixture was stirred at room temperature under normal pressure overnight under a hydrogen atmosphere. The reaction solution was filtered and the filtrate was evaporated, to give 379 mg of the title compound as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06784192B2
Source datasetuspto-grants-2004_08
ORD IDord-190692121f9c41ccaa538315c167db0e
Source noteuspto-grants-2004_08