HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22678362, compound → HCID 22678736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22678362 | HCID 22678362 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22678736 | HCID 22678736 | 98.4% |
Reaction Steps
554 mg of 1-(benzyloxycarbonyl)-4-[(E)-2-[(2-cyclohexylmethyloxy)phenyl]-1-ethenyl]piperidine was dissolved in 10 ml of ethanol, 250 mg of 10% palladium-carbon powder (water-containing product) was added thereto, and the mixture was stirred at room temperature under normal pressure overnight under a hydrogen atmosphere. The reaction solution was filtered and the filtrate was evaporated, to give 379 mg of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06784192B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-190692121f9c41ccaa538315c167db0e |
| Source note | uspto-grants-2004_08 |