HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22678421, compound → HCID 22678656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22678421 | HCID 22678421 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22678656 | HCID 22678656 | 70% |
Reaction Steps
332 mg of 1-[(2-methoxy-3-pyridyl)methyl]-4-[(E)-2-(2-pyridyl)-1-ethenyl]piperidine obtained in Example 29 and 79 mg of 10% palladium-carbon powder (water-containing product) were suspended in 5 ml of ethanol. After replacing the atmosphere of a container with hydrogen, the mixture was stirred at normal temperature under normal pressure for 30 minutes. The reaction solution was filtered, and the filtrate was evaproated, to give 234 mg of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06784192B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-c69675b1200b4f919afd7c61dde37392 |
| Source note | uspto-grants-2004_08 |