Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1837725Generated: November 2, 2026

HCID 22678421, compound → HCID 22678656, compound

https://huagongshe.com/reaction/1837725

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22678421HCID 22678421—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 22678656HCID 2267865670%

Reaction Steps

332 mg of 1-[(2-methoxy-3-pyridyl)methyl]-4-[(E)-2-(2-pyridyl)-1-ethenyl]piperidine obtained in Example 29 and 79 mg of 10% palladium-carbon powder (water-containing product) were suspended in 5 ml of ethanol. After replacing the atmosphere of a container with hydrogen, the mixture was stirred at normal temperature under normal pressure for 30 minutes. The reaction solution was filtered, and the filtrate was evaproated, to give 234 mg of the title compound as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06784192B2
Source datasetuspto-grants-2004_08
ORD IDord-c69675b1200b4f919afd7c61dde37392
Source noteuspto-grants-2004_08