HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 53723112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 53994143 | HCID 53994143 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53723112 | HCID 53723112 | — |
Reaction Steps
To a solution of 11-9 (0.4037 mmol) in EtOH (3 mL) was added 1N NaOH (0.600 ml, 0.600 mmol). After stirring for 2 h, the solvents were evaporated and the residue was chromatographed (silica gel, 20:10:1:1 to 10:10:1:1 ethyl acetate/EtOH/water/NH4OH) to give 11-10 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06784190B2 |
| Source dataset | uspto-grants-2004_08 |
| ORD ID | ord-f986c0b21d6741f293c1e625a9a33b18 |
| Source note | uspto-grants-2004_08 |