Vanillin → HCID 18753047, compound

HRID 1838123Notes

Reaction equation

[C:1]([O:4][CH2:5][CH3:6])(=[O:3])C.[O:7]=[CH:8][C:9]1[CH:17]=C[C:14](O)=[C:11](OC)[CH:10]=1.Cl[CH2:19]Cl>>[CH3:19][O:3][CH2:1][O:4][CH2:5][C:6]1[CH:17]=[C:9]([CH2:8][OH:7])[CH:10]=[CH:11][CH:14]=1

Participants

Reactant 3

HCID 1183Vanillin

HCID 6344Dichloromethane

HCID 8857Ethyl Acetate

Product 1

HCID 18753047HCID 18753047, compound

Procedure

1H NMR (CDCl3) δ2.03, 3.41, 4.59, 4.68, 4.70, 7.3 ppm. TLC Rf 0.36 (1:1 ethyl acetate in dichloromethane, vanillin staining).

Sources & evidence

ORD record: ord-cb6cd915d74748baa0e19e42f0144075
Source dataset: uspto-grants-2004_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06673793B2

Reaction notes

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