HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15521776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 10116033 | HCID 10116033 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15521776 | HCID 15521776 | — |
Reaction Steps
The compound of Example 56 is treated with aqueous formaldehyde and sodium borohydride. The compound obtained is salified with a solution of hydrochloric acid in diethyl ether. The hydrochloride is then isolated after filtration and drying at 45° C. under reduced pressure; M.p.=156° C. (HCl.1.5H2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673790B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-db2dd9dcb6fd408389367c3a2affacad |
| Source note | uspto-grants-2004_01 |