HuagongsheHuagongshe Chemistry Print Report · For research reference only
Uracil → Benzyl chloromethyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Uracil | HCID 1174 | — |
| Reactant | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| Reactant | Thieno(3,2-d)pyrimidine-2,4(1H,3H)-dione | HCID 7059273 | — |
| Product | Benzyl chloromethyl ether | HCID 137983 | — |
Reaction Steps
In a similar manner to the procedures described in Reference Example 3, reactions were carried out using thieno[3,2-d]pyrimidine-2,4-dione, instead of pyrimidine-2,4-dione, and using 2-(trimethylsilyl)ethoxymethyl chloride, instead of benzyloxymethyl chloride, to give the title compound (yield 87%) as a pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673804B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-c7311b8f29934c51857a3b78011c9de9 |
| Source note | uspto-grants-2004_01 |