HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10945066, compound → HCID 10857172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10945066 | HCID 10945066 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 10857172 | HCID 10857172 | — |
Reaction Steps
treating 1-hydroxy-8-nitro-6H-benzo[c]chromen-6-one with a second transition metal catalyst under a hydrogen atmosphere at a pressure of about 20 to about 60 psi, preferably about 40 psi, in a third solvent, preferably N-methylpyrrolidin-2-one (NMP) at a concentration of about 0.5M to about 1.0M, preferably 0.7M, to provide 8-amino-1-hydroxy-6H-benzo[c]chromen-6-one in NMP;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673930B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-d7a24758a73a420ea47c769db0fbe5b0 |
| Source note | uspto-grants-2004_01 |