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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1838670Generated: November 3, 2026

HCID 10945066, compound → HCID 10857172, compound

https://huagongshe.com/reaction/1838670

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10945066HCID 10945066—
SolventN-methyl-2-pyrrolidoneHCID 13387—
ProductHCID 10857172HCID 10857172—

Reaction Steps

treating 1-hydroxy-8-nitro-6H-benzo[c]chromen-6-one with a second transition metal catalyst under a hydrogen atmosphere at a pressure of about 20 to about 60 psi, preferably about 40 psi, in a third solvent, preferably N-methylpyrrolidin-2-one (NMP) at a concentration of about 0.5M to about 1.0M, preferably 0.7M, to provide 8-amino-1-hydroxy-6H-benzo[c]chromen-6-one in NMP;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06673930B2
Source datasetuspto-grants-2004_01
ORD IDord-d7a24758a73a420ea47c769db0fbe5b0
Source noteuspto-grants-2004_01