HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 178518927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 178518919 | HCID 178518919 | — |
| Product | HCID 178518927 | HCID 178518927 | 75% |
Reaction Steps
4,5-Dichloro-3-hydroxypyridazine (25.0 g; 0.151 mol) was dissolved in piperidine (120 mol), under reflux condition for 24 hours. After cooling, the deposited crystal was filtered, to give 4,5-dipiperidino-3-hydroxypyridazine in white crystal (30.3 g as a yield of 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06676932B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-661323e83da64554862a1abf172855a0 |
| Source note | uspto-grants-2004_01 |