HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 131724289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2,3-Epoxypropyl 4'-methoxyphenyl ether | HCID 16646 | — |
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Product | HCID 131724289 | HCID 131724289 | — |
Reaction Steps
Epoxide 6 (1.0 g, 5.5 mmol) and Boc-ethylenediamine (0.88 g, 5.5 mmol) were dissolved in 20 mL EtOH and the mixture was heated at reflux for 24 h. The solvent was evaporated and the residue was purified using column chromatography (1:1, Hex:EtOAc) to afford compound 11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06677336B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-c9e9228e5bcb49dfa28f3b7fb5d9b6f0 |
| Source note | uspto-grants-2004_01 |