Phenylacetic Acid → HCID 10155740, compound

HRID 1838932Notes

Reaction equation

HRID 1838932 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[C:3]=1[NH:9][C:10](=[O:30])[CH2:11][N:12]1[CH2:17][CH2:16][N:15]([C:18](=[O:29])C(O)CCC2C=CC=CC=2)[CH2:14][CH2:13]1.[C:31]1([CH2:37]C(O)=O)[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1.OC1C=CC=CC=1[C@@H](CC)C(O)=O>>[CH3:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([CH3:1])[C:3]=1[NH:9][C:10](=[O:30])[CH2:11][N:12]1[CH2:13][CH2:14][N:15]([C:18](=[O:29])[CH2:37][C:31]2[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=2)[CH2:16][CH2:17]1

Participants

4

Reactant 3

HCID 999Phenylacetic AcidHCID 12985297HCID 12985297, compoundHCID 69892093HCID 69892093, compound

Product 1

HCID 10155740HCID 10155740, compound

Procedure

Compound 14 was prepared in the manner of compound 7 substituting 2-phenylacetic acid for (R)-2-hydroxy-phenylbutyric acid in part C to afford compound 14: Mass spectrum (M+1)=366.40.

Sources & evidence

ORD record
ord-c2b0895b462e48e793ab781aadbcb764
Source dataset
uspto-grants-2004_01
Patent number
US06677343B2

Reaction notes

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