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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1838985Generated: October 30, 2026

HCID 22347442, compound → HCID 9907963, compound

https://huagongshe.com/reaction/1838985

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22347442HCID 22347442—
ReactantHCID 22347460HCID 22347460—
ProductHCID 9907963HCID 990796316%

Reaction Steps

400 mg (1.40 mmol) of 3-t-butoxycarbonylamino-4-methoxybenzenesulfonamide and 533 mg (1.40 mmol) of benzyl 4-chloro-2-N-phenoxycarbonylanthranilate were treated in the same way as in Preparation Example 17 to obtain 86 mg (yield 16%: 4 steps) of the above-identified compound. Properties: colorless crystal, Melting point: >200° C. (decomposition), PMR (δ ppm, DMSO-d6): 3.81 (3H, s), 7.26-7.37 (5H, m), 7.77 (1H, s), 7.90 (1H, d), 7.94 (1H, d), 11.73 (1H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06677344B2
Source datasetuspto-grants-2004_01
ORD IDord-aa81a87e62e0464289389d84e59276e2
Source noteuspto-grants-2004_01